Estimation Of Hardness Of Water Ii Edta Complexometric Titration Ii M 1 = mgso4 molarity m 2 = edta molarity. v 1 = volume of mgso4 v 2 = volume of edta consumed. m 1 v 1 = m 2 v 2. m 2 = m 1 v 1 v 2. step iii. standardization of permanent hardness of water :pipette out 100ml of hard water sample into a beaker containing 250ml and boil the water till volume reduces to 50ml (all the bicarbonates of ca 2 , mg 2 decomposes tocaco3and mg(oh) 2 respectively). You will use edta complexometric titration to determine the hardness of a sample of water brought from your home. both the total hardness and the individual calcium and magnesium hardnesses will be measured. edta and the metallochromic indicators used are involved in complexation reactions with the magnesium and calcium ions that are.
Unit 1 Estimation Of Hardness Of Water By Edta Method Youtube Hardness is commonly expressed as caco3 in mg l. the degree of hardness of drinking water has been classified in terms of the equivalent caco3 concentration as follows: soft 0 60 mg l; medium 60 120 mg l; hard 120 180 mg l; very hard 180 mg l; although hardness is caused by cation, it may also be discussed in terms of carbonate (temporary) and. Filter through filter paper to remove insoluble caco3 and mgco3. make up the volume to the original 100 ml by adding distilled water. now pipette out 20 ml of this solution into a clean conical flask. then repeat the process of titration steps as mentioned above. let the burette reading of edta be v4 ml. Estimation of hardness of water by edta. At a ph of 3 the cay 2– complex is too weak to successfully titrate. (b) titration of a 50.0 ml mixture of 0.010 m ca 2 and 0.010 m ni 2 at a ph of 3 and a ph of 9 using 0.010 m edta. at a ph of 3 edta reacts only with ni 2 . when the titration is complete, raising the ph to 9 allows for the titration of ca 2 .
Publication 2 2630 250 Estimation Of Hardness Of Water By Edta Method Estimation of hardness of water by edta. At a ph of 3 the cay 2– complex is too weak to successfully titrate. (b) titration of a 50.0 ml mixture of 0.010 m ca 2 and 0.010 m ni 2 at a ph of 3 and a ph of 9 using 0.010 m edta. at a ph of 3 edta reacts only with ni 2 . when the titration is complete, raising the ph to 9 allows for the titration of ca 2 . 1. determination of alkalinity in the given water sample. 2. determination of temporary and permanent hardness in water sample using edta as standard solution. 3. determination of available chlorine in bleaching powder. 4. determination of chloride content in water sample by mohr’s method. 5. It is also not good for fish tanks. in general, there are many applications where ability to easily determine water hardness is very important. complexometric titration is one of the best ways of measuring total water hardness. at ph around 10 edta easily reacts with both calcium and magnesium in the same molar ratio (1:1).